Chapter 5 GLC
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ID： |
AD2718F018194B149B71513D15AD5C66 |
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文件大小(MB)： |
0.35 |
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页数： |
90 |
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文件格式： |
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日期： |
2002-6-11 |
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购买： |
文本摘录（文本识别可能有误，但文件阅览显示及打印正常，pdf文件可进行文字搜索定位）：
Transmittal No. 96-E1 (9/96),Form FDA 2905a (6/92),Pesticide Analytical Manual Vol. I SECTION 500,500–1,Table of Contents,page date,501: General Information,501 A: Principles 501-1 1/94,501 B: Equipment for GLC 501-1 1/94,Gas Chromatographic Components 501-1 1/94,Other Apparatus 501-2 1/94,Reagents and Gases 501-3 1/94,501 C: Residue Methodology for GLC Determination 501-3 1/94,Cleanup 501-4 1/94,Reagent Blanks 501-5 1/94,Choice of Solvent 501-6 1/94,501 D: Injection Techniques 501-6 1/94,Manual Injection 501-6 1/94,Autoinjectors 501-7 1/94,501 E: Reference Standards 501-8 1/94,References 501-8 1/94,Chapter 1,Regulatory Operations,Chapter 2,General Analytical,Operations and Information,Chapter 3,Multiclass,MRMs,Chapter 5,GLC,Chapter 4,Selective,MRMs,Chapter 6,HPLC,Transmittal No. 96-E1 (9/96),500–2 Form FDA 2905a (6/92),SECTION 500 Pesticide Analytical Manual Vol. I,page date,502: Columns,502 A: Introduction 502-1 1/94,Column Specifications 502-1 1/94,Column Parameters 502-2 1/94,502 B: Packed Columns 502-6 1/94,Components of Packed Columns 502-6 1/94,Preparation of Packed Columns 502-8 1/94,Installation of Packed Columns 502-9 1/94,Conditioning of Packed Columns 502-10 1/94,Rejuvenation of Packed Columns 502-10 1/94,Criteria for Acceptable Packed Columns 502-11 1/94,Recommended Operating Procedures 502-12 1/94,for Packed Columns,502 C: Open Tubular Capillary Columns 502-13 1/94,Column Description 502-14 1/94,Injection onto Capillary Columns 502-16 1/94,Capillary Column Systems 502-16 1/94,Installation and Conditioning of 502-20 1/94,Capillary Columns,Rejuvenation of Capillary Columns 502-21 1/94,Recommended Operating Procedure for 502-22 1/94,Wide Bore Columns (Isothermal),Apparatus and Reagents 502-22 1/94,System Startup and Inspection 502-25 1/94,References 502-25 1/94,503: Detectors,503 A: Introduction 503-1 1/94,Definitions of Detector Characteristics 503-1 1/94,503 B: Electron Capture Detector 503-2 1/94,Principles 503-3 1/94,Design 503-3 1/94,Apparatus and Reagents 503-3 1/94,Detector Characteristics 503-4 1/94,Other Influences on Detector Performance 503-7 1/94,Recommended Operating Procedures 503-8 1/94,503 C: Flame Photometric Detector 503-9 1/94,Principles 503-9 1/94,Design 503-9 1/94,Apparatus and Reagents 503-10 1/94,Detector Characteristics 503-10 1/94,Other Influences on Detector Performance 503-11 1/94,Recommended Operating Procedures 503-12 1/94,Troubleshooting 503-13 1/94,503 D: Electrolytic Conductivity Detector 503-14 1/94,Principles 503-14 1/94,Transmittal No. 96-E1 (9/96),Form FDA 2905a (6/92),Pesticide Analytical Manual Vol. I SECTION 500,500–3,page date,Design 503-14 1/94,ElCD-X 503-16 1/94,Principles 503-16 1/94,Apparatus and Reagents 503-16 1/94,Detector Characteristics 503-17 1/94,Other Influences on Detector Performance 503-19 1/94,Recommended Operating Procedures 503-21 1/94,System Suitability Test 503-21 1/94,Troubleshooting 503-22 1/94,ElCD-N 503-23 1/94,Principles 503-23 1/94,Apparatus and Reagents 503-23 1/94,Detector Characteristics 503-23 1/94,Other Influences on Detector Performance 503-24 1/94,Recommended Operating Procedures 503-25 1/94,System Suitability Test 503-25 1/94,Troubleshooting 503-25 1/94,General Precautions for ElCDs 503-26 1/94,Apparatus and Reagents 503-28 1/94,Detector Characteristics 503-28 1/94,Other Influences on Detector Performance 503-30 1/94,Recommended Operating Procedures 503-31 1/94,References 503-32 1/94,504: Quantitation,504 A: Introduction 504-1 1/94,504 B: Manual Quantitation 504-2 1/94,Measurement of Peak Height 504-2 1/94,Measurement of Area by Triangulation 504-2 1/94,504 C: Electronic Integration 504-3 1/94,504 D: Special Considerations for Complex 504-6 1/94,Chromatograms,BHC 504-6 1/94,Chlordane 504-8 1/94,PCBs 504-10 1/94,Toxaphene 504-14 1/94,References 504-15 1/94,505: Bibliography,General Texts 505-1 1/94,Inlets 505-1 1/94,Columns 505-1 1/94,Detectors 505-1 1/94,Transmittal No. 96-E1 (9/96),500–4 Form FDA 2905a (6/92),SECTION 500 Pesticide Analytical Manual Vol. I,page date,Figures,502-a Polysiloxane Stationary Phases 502-2 1/94,502-b GLC Column Parameters 502-4 1/94,502-c Ferrules for Connecting Glass and Metal 502-9 1/94,502-d Capillary Column Cross-Section 502-15 1/94,502-f Van Deemter Curves 502-19 1/94,502-g Capillary Column Inlet System 502-23 1/94,503-a Two EC Detector Designs 503-3 1/94,503-b Reproducibility 503-5 1/94,503-c Dynamic Response Ranges 503-6 1/94,503-d Linear Response Range 503-6 1/94,503-f Effect of Carrier Gas Flow Rate 503-7 1/94,503-g Single-Flame FPD 503-9 1/94,503-h Dual-Flame FPD 503-10 1/94,503-i Block Diagram of the ElCD 503-15 1/94,503-j ElCD Reactor and Conductivity ……
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